Standard Specification for Reclaimed Methylene Chloride

ABSTRACT
This specification covers reclaimed methylene chloride used in various industries for noncritical applications. Tests for specific gravity, acidity, water content, appearance, color, nonvolatile residue, chloride content, assay, and 1,1,1-trichloroethane content shall be performed and shall conform to the requirements specified.
SCOPE
1.1 This specification covers the grade of methylene chloride typically needed in various industries for noncritical applications, such as in paint stripping formulations. It may be used as a reference document by purchasers or by persons establishing in-house methylene chloride recovery programs.  
1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Jul-2023
Drafting Committee
D26.02 - Vapor Degreasing

Relations

Effective Date
01-Jan-2024
Effective Date
01-Apr-2020
Effective Date
01-Apr-2020
Effective Date
01-Apr-2020
Effective Date
01-Jan-2020
Effective Date
01-Jun-2015
Effective Date
01-Jun-2015
Effective Date
01-Jun-2015
Effective Date
01-Jun-2015
Effective Date
01-Mar-2012
Effective Date
01-Mar-2012
Effective Date
01-Aug-2011
Effective Date
01-Aug-2011
Effective Date
01-Jun-2010
Effective Date
01-Feb-2010

Overview

ASTM D5395-03(2023), Standard Specification for Reclaimed Methylene Chloride, sets comprehensive requirements for reclaimed methylene chloride (also known as dichloromethane, MeCl, or MCL) used primarily in noncritical industrial applications. Published and maintained by ASTM International, this standard ensures reclaimed methylene chloride is suitable for product safety and consistent performance by specifying key physical and chemical properties, quality parameters, and regulatory compliance. This specification is widely recognized across industries such as paint stripping, cleaning, and solvent recycling programs.

Key Topics

  • Purpose and Scope

    • Addresses quality and suitability for noncritical uses of reclaimed methylene chloride.
    • Intended for use in procurement, manufacturing, and quality assurance-especially for industrial buyers and companies running in-house solvent recovery.
  • Physical and Chemical Properties
    The following properties are critical for compliance:

    • Specific gravity (at 25/25°C)
    • Acidity (as HCl)
    • Water content
    • Appearance and clarity
    • Color (Pt-Co scale)
    • Nonvolatile residue
    • Chloride content
    • Assay (purity percentage)
    • 1,1,1-Trichloroethane content
  • Testing and Methods

    • Explicit references to standardized ASTM testing methods for each quality attribute, such as D2111 for specific gravity and D2109 for nonvolatile matter.
    • Requires packaging and labeling compliance according to federal transportation (49 CFR 100-199) and workplace safety (29 CFR 1910.1200) regulations.
  • Regulatory Alignment

    • Developed under the World Trade Organization (WTO) Technical Barriers to Trade (TBT) Committee principles, enabling international relevance.
    • Alignment with US DOT and OSHA regulations for packaging, hazard communication, and shipping of hazardous materials.

Applications

  • Paint Stripping Formulations
    Reclaimed methylene chloride is frequently used in the production of paint strippers, where high purity is not critical but reliable solvent performance is required.

  • In-house Solvent Recovery
    Organizations establishing solvent reclamation programs use the standard as a benchmark to qualify recovered methylene chloride for reuse, ensuring cost savings and environmental compliance.

  • General Solvent Use
    Enables safe and consistent use of reclaimed methylene chloride in cleaning agents, adhesives, and degreasing operations where noncritical performance requirements are met.

  • Purchasing and Procurement
    Purchasing departments utilize ASTM D5395-03(2023) to specify acceptable reclaimed methylene chloride quality for industrial supply contracts.

Related Standards

  • ASTM D2108 - Standard Test Method for Color of Halogenated Organic Solvents
  • ASTM D2109 - Methods for Nonvolatile Matter in Halogenated Organic Solvents
  • ASTM D2111 - Methods for Specific Gravity and Density of Halogenated Organic Solvents
  • ASTM D2988 - Test Methods for Water-Soluble Halide Ions
  • ASTM D2989 - Test Method for Acidity-Alkalinity
  • ASTM D3401, E1064 - Test Methods for Water Content
  • ASTM D3741 - Test Method for Appearance
  • ASTM D6806 - Practice for Analysis by Gas Chromatography
  • 49 CFR 100-199 - US DOT Hazardous Materials Regulations
  • 29 CFR 1910.1200 - OSHA Hazard Communication Standard

By adhering to ASTM D5395-03(2023), users can confidently specify, recover, or purchase reclaimed methylene chloride that meets recognized safety, quality, and performance metrics, ensuring responsible handling in a wide range of industrial environments.

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ASTM D5395-03(2023) - Standard Specification for Reclaimed Methylene Chloride

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Frequently Asked Questions

ASTM D5395-03(2023) is a technical specification published by ASTM International. Its full title is "Standard Specification for Reclaimed Methylene Chloride". This standard covers: ABSTRACT This specification covers reclaimed methylene chloride used in various industries for noncritical applications. Tests for specific gravity, acidity, water content, appearance, color, nonvolatile residue, chloride content, assay, and 1,1,1-trichloroethane content shall be performed and shall conform to the requirements specified. SCOPE 1.1 This specification covers the grade of methylene chloride typically needed in various industries for noncritical applications, such as in paint stripping formulations. It may be used as a reference document by purchasers or by persons establishing in-house methylene chloride recovery programs. 1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT This specification covers reclaimed methylene chloride used in various industries for noncritical applications. Tests for specific gravity, acidity, water content, appearance, color, nonvolatile residue, chloride content, assay, and 1,1,1-trichloroethane content shall be performed and shall conform to the requirements specified. SCOPE 1.1 This specification covers the grade of methylene chloride typically needed in various industries for noncritical applications, such as in paint stripping formulations. It may be used as a reference document by purchasers or by persons establishing in-house methylene chloride recovery programs. 1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D5395-03(2023) is classified under the following ICS (International Classification for Standards) categories: 71.080.20 - Halogenated hydrocarbons. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM D5395-03(2023) has the following relationships with other standards: It is inter standard links to ASTM E1064-24, ASTM D2988-96(2020), ASTM D2111-10(2020), ASTM D3741-00(2020), ASTM D2108-10(2020), ASTM D2111-10(2015), ASTM D2108-10(2015), ASTM D2988-96(2015), ASTM D3741-00(2015)e1, ASTM D6806-02(2012), ASTM D3401-97(2012), ASTM D2989-01(2011), ASTM D2109-01(2011), ASTM D2988-96(2010), ASTM D2108-10. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM D5395-03(2023) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D5395 − 03 (Reapproved 2023)
Standard Specification for
1,2
Reclaimed Methylene Chloride
This standard is issued under the fixed designation D5395; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D2989 Test Method for Acidity-Alkalinity of Halogenated
Organic Solvents and Their Admixtures
1.1 This specification covers the grade of methylene chlo-
D3401 Test Methods for Water in Halogenated Organic
ride typically needed in various industries for noncritical
Solvents and Their Admixtures
applications, such as in paint stripping formulations. It may be
D3741 Test Methods for Appearance of Admixtures Con-
used as a reference document by purchasers or by persons
taining Halogenated Organic Solvents
establishing in-house methylene chloride recovery programs.
D6806 Practice for Analysis of Halogenated Organic Sol-
1.2 This international standard was developed in accor-
vents and Their Admixtures by Gas Chromatography
dance with internationally recognized principles on standard-
E1064 Test Method for Water in Organic Liquids by Coulo-
ization established in the Decision on Principles for the
metric Karl Fischer Titration
Development of International Standards, Guides and Recom-
2.2 U.S. Government Documents:
mendations issued by the World Trade Organization Technical
29 CFR 1910.1200 Department of Labor, OSHA Regula-
Barriers to Trade (TBT) Committee.
tions on Hazard Communications
49 CFR 100 to 199 Department of Transportation Hazardous
2. Referenced Documents
Materials Regulations
2.1 ASTM Standards:
D2108 Test Method for Color of Halogenated Organic
3. Properties
Solvents and Their Admixtures (Platinum-Cobalt Scale)
3.1 Reclaimed methylene chloride shall meet the require-
D2109 Test Methods for Nonvolatile Matter in Halogenated
ments of Table 1.
Organic Solvents and Their Admixtures
D2111 Test Methods for Specific Gravity and Density of
4. Packaging and Package Marking
Halogenated Organic Solvents and Their Admixtures
4.1 Package and label industrial or commercial quantities in
D2988 Test Methods for Water-Soluble Halide Ion in Halo-
accordance with DOT regulations as found in 49 CFR 100 to
genated Organic Solvents and Their Admixtures
199, and in accordance with state and local regulations, and
with OSHA regulations found in 29 CFR 1910.1200.
This specification is under the jurisdiction of ASTM Committee D26 on
Halogenated Organic Solvents and Fire Extinguis
...

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