ISO/PRF TS 21596
(Main)Solid biofuels -- Determination of grindability -- Hardgrove type method for thermally treated biomass fuels
Solid biofuels -- Determination of grindability -- Hardgrove type method for thermally treated biomass fuels
Biocombustibles solides -- Détermination de la broyabilité -- Méthode de type Hardgrove pour les combustibles de biomasses traitées thermiquement
General Information
Standards Content (sample)
TECHNICAL ISO/TS
SPECIFICATION 21596
First edition
Solid biofuels — Determination
of grindability — Hardgrove type
method for thermally treated biomass
fuels
PROOF/ÉPREUVE
Reference number
ISO/TS 21596:2021(E)
ISO 2021
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ISO/TS 21596:2021(E)
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ISO/TS 21596:2021(E)
Contents Page
Foreword ........................................................................................................................................................................................................................................iv
Introduction ..................................................................................................................................................................................................................................v
1 Scope ................................................................................................................................................................................................................................. 1
2 Normative references ...................................................................................................................................................................................... 1
3 Terms and definitions ..................................................................................................................................................................................... 1
4 Principle ........................................................................................................................................................................................................................ 2
5 Apparatus ..................................................................................................................................................................................................................... 2
5.1 Standard HGI mill ................................................................................................................................................................................. 2
5.2 Sieves ............................................................................................................................................................................................................... 2
5.3 Glass measuring cylinder ............................................................................................................................................................... 2
5.4 Sieving machine ..................................................................................................................................................................................... 3
5.5 Balance ........................................................................................................................................................................................................... 3
5.6 Cutting mill ................................................................................................................................................................................................. 3
6 Sampling and sample preparation .................................................................................................................................................... 3
6.1 General ........................................................................................................................................................................................................... 3
6.2 Moisture conditions ............................................................................................................................................................................ 3
6.3 Pre-grinding and sieving ................................................................................................................................................................ 3
6.4 Sample size ................................................................................................................................................................................................. 3
7 Procedure..................................................................................................................................................................................................................... 3
8 Calculation .................................................................................................................................................................................................................. 4
9 Reproducibility ...................................................................................................................................................................................................... 5
10 Test report ................................................................................................................................................................................................................... 5
Annex A (normative) Calibration curve and Thermally Treated Biomass Grindability Index
(TTBGI) values for the reference materials ............................................................................................................................. 6
Bibliography ................................................................................................................................................................................................................................ 9
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ISO/TS 21596:2021(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
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ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/ patents).Any trade name used in this document is information given for the convenience of users and does not
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expressions related to conformity assessment, as well as information about ISO's adherence to the
World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www .iso .org/
iso/ foreword .html.This document was prepared by Technical Committee ISO/TC 238 Solid biofuels.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www .iso .org/ members .html.iv PROOF/ÉPREUVE © ISO 2021 – All rights reserved
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ISO/TS 21596:2021(E)
Introduction
Grindability characteristics are of fundamental importance during solid biofuel preparation for energy
conversion processes, requiring a predictable particle size distribution. Particles that are too large or
too wide in their distribution may result in feeding problems as well as un-burnt fuel passing through
the conversion process. Also, in case of processing of biomass for pre-treatment, consistency in particle
size determines the yield of such pre-treatment as well as the quality of the final solid biofuel.
The effectiveness of combustion in a pulverized fuel furnace depends strongly on the reactivity and
particle size distribution of the pulverized fuel among other factors. For coal, the Hardgrove Grindability
Index (HGI) test was developed to characterize the relative grindability of a particular quality of coal
relative to a pre-determined standard quality of coal (ASTM D 409). The HGI test is an empirical batch
method that simulates the continuous grinding and crushing operation of a ball, table or tube type of
industrial coal pulverizer, herein also called coal mill. The HGI value is an indication of the degree of
grinding required to reach a particular particle size necessary for effective combustion.
Manufacturers of coal pulverizers for preparation of pulverized coal for combustion in coal burning
plants provide curves that show the relationships between the HGI for coal, coal mill capacity in terms
of tonne/h and coal mill power in kW. This is done as part of the boiler contract and guarantees. It
also serves as a first indication as to how to operate a mill when pulverizing different coals with
predetermined standard properties. A HGI of 50, which is standard industry convention, implies that
100 % capacity in tonnes per hour (as indicated) can be reached for the coal at a fineness of 70 % less
than 75 microns and 99,5 % less than 300 microns. So, if a coal has a HGI of less than 50 it implies
some level of pulverizer capacity loss while on the other hand, a HGI higher than 50 indicates some
level of pulverizer capacity gain. The HGI method is internationally accepted and quoted as part of the
specification of coal for international trade.Grindability may also be applied to thermally pre-treated compressed biomass materials, such as
pellets, for pulverization in coal mills. Pre-treatment methods for biomass fuels such as torrefaction,
steam treatment or hydro-thermal carbonization (HTC) upgrade the properties of biomass making it
more effective as a fuel. With increasing interest in the use of such pre-treated biomass fuels for direct
co-firing applications in conventional pulverized coal boilers, this method herein describes a laboratory
procedure for determination of the grindability of pre-treated biofuels for powder fuel preparation.
The HGI determination is subject to many limitations, including the fact that measurements can be
insensitive to the heterogeneous properties of coal that arise from different mineral contents, maceral
constituents and levels of maturity. Three relevant adaptations are applied to the standard HGI method
in order to extend its applicability to thermally pre-treated biomass fuels. The adaptations and their
justification are as follows:— Amount of sample used for the test determination.
— Particle size used as basis for defining grindability.
— Reference materials for establishing the calibration curve.
0.1 Amount of the sample used for test determination
Coal pulverizers are volumetric devices but with the densities of coals being fairly similar, the capacity
of these devices is expressed in mass units per hour. In contrast different biomass materials have
different densities. Therefore, the sample amount was changed to the volume (75 ± 0,5) cm of input
material, which approximates the bulk volume of the standard reference coal samples with a particle
size between 1,18 mm and 600 μm.0.2 Particle size used as basis for defining grindability
The standard HGI test for coal uses the mass of particles passing a sieve with an aperture size of 75 μm
as criteria for determining the grindability and the resulting HGI value. The furnace volume is designed
from the knowledge of coals to be utilized so as to provide an adequate residence time for complete
combustion. Combustion efficiency depends in part on fuel particle size especially for pulverized coal
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ISO/TS 21596:2021(E)
furnaces. As the combustion efficiency also depends on the reactivity, which is linked to volatile matter
content of fuels, the particle size for high-volatile fuels, such as thermally treated biomass, would not
necessarily need to meet the strict fineness requirements for coal powders. Therefore, a sieve with an
aperture size of 500 μm is used for determination of grindability of thermally treated biomass. This
adaptation also has positive implications on the repeatability of the determination.
0.3 Reference materials for establishing the calibration curveIn the standard HGI test for coal, four references coals are needed for calibrating a HGI mill. This enables
reproducibility of the results across different labs. For the thermally treated biomass grindability
index determination, this is the very first step. The thermally treated biomass grindability index is
an index for materials originating from biomass. The sieving behavior of biomass materials differs
fundamentally from that of coals due to the difference in the sphericity of the coal particles. Biomass
materials, including thermally treated biomass, are more fibrous and have lengthy dust particles
compared to coals. Thermal treatment processes, such as torrefaction, modifies the property of biomass
by making biomass more like charcoal. Woody charcoal is a product of slow pyrolysis, which degrades
the fibrous nature of the biomass. This consequently improves its grindability as well as the sphericity
of the pulverized fuel.The adapted grindability method uses wood pellets (ISO 17225-2:2021 A1 class pellets) and wood
based charcoal (ISO 17225-1:2021 Table 14) as calibration reference materials. These biomass reference
materials will be given assigned Thermally Treated Biomass Grindability Index (TTBGI) values as a
result of the procedures described in the Annex A. The materials are available commercially for the
determination.vi PROOF/ÉPREUVE © ISO 2021 – All rights reserved
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TECHNICAL SPECIFICATION ISO/TS 21596:2021(E)
Solid biofuels — Determination of grindability —
Hardgrove type method for thermally treated biomass
fuels
1 Scope
This document describes a method for determination of grindability of graded thermally treated and
densified biomass fuels such as classified in ISO/TS 17225-8, for the purpose of preparing fuels with a
defined particle size distribution for e...
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